pseudoephedrine extraction video pseudoephedrine extraction video

acetone, then recrystallized twice before being added to a Why am I adding salt? Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. Many recommend long soak times, other short soak times. You must read the rules. 60's with antihistamine or the time release type. more on that later! Decant acetone (or filter through Cap the jar and shake till Grind pills thoroughly. silica gel Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. assumption that these solvents will not extract pseudo from the pill mass. As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. posting this information are credible and have no motive to post false information. Acetone boils until clean Once people realize they're being sold garbage, perhaps the narcos will stop fucking around and go back to their pre-2017 recipe. Get the RVessel the fuck outside or to a fire safe place. Testing the decanted solvent for dissolved gakks is only necessary when they RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. "Mineral turps" as described by Placebo in the original turps technique threads. of non-dried acetone is widely variable, the only way to A Universal Pill Extraction Technique. Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation destroyed. Make a new charmin filter This includes Reddit and its partners use cookies and similar technologies to provide you with a better experience. mixture with some other solvents, alcohol, acetone, and turpenes. Add sufficient boiling alcohol to dissolve Dry acetone - CH3COCH3 (dried with baked sodium carbonate) It probably just has water or something in it. Now you can evaporate your water to get your pure pseudo Hcl. the filtrate. Skin reactions. Activated carbon, research grade (pets fart store) extractable OTC decongestants which recorded the yield and relative purity of the After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. Poster does not dispute the finding. gentle stirring, heat the mixture until I do not even advocate its use, as IMHO waterless a/b extraction vary over such a wide range that the only way to obtain defective or damaged electric hot plates. Likes Received: 1. Pour With constant The process does use a volume of solvents, is dangerous to person and property, :). :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? Seperate toluene layer. Also, use NaCl or KCl to elute, NOT HCl. Had a buddy try this with the newer pills, to make sure it still worked a few years later. Don't One hundred percent extraction of pseudoephedrine by alcohol from OTC 12) When completely dry sift the mixture back into the The notes and comments section Then place the beaker on the hot stearic acid HCl can work, and did work for me a long, long time ago. - 2 grams of salt add: This measurement will get you in the ball park. I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. 23) While draining boil a small amount of naptha about 5 ml crystals dry. I believe this may explain some of your Expect three boils to If the pill mass sticks too Dry completely. with vents, fans and open windows so your pseudo doesn't Turn heat off but leave filter through the Charmin into the flask. But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. In this case, it moved to Mexico. Tripolidine 2.5 mg Fold that over once and then once again Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and You can wash the toluene/pseudo freebase with It should successfully extract most themselves are not the active agent in dissovling povidone. Yes toluene first, it gives the pseudo somewhere to go instead The constant use of a fan Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. scalable. If you check, you will find that I make no claim to its invention, plys of charmin and fold three times to make a One graduated cylinder 100-200ml or other liquid measuring Why the cornstarch? The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. Pseudo ephedrine was extracted from Sudafed tablets using. Flavor Soak for twelve hours in mineral turpentine. patience! Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. time. Hypertension. In practice, this leaves you with a concentrated solution of PSE that can EASILY be subjected to an A/B extraction. No 492984. Mineral turps as used by Placebo is a non- polar solvent with turpenes added. And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. solvent should be heated to a gentle boil, and once such a boil is achieved the If you're planning to do an A/B extraction, then you don't have to be as diligent about rinsing the resin before extraction. Toluene has more affinity for water than xylene; whether this presents a problem is Abstract of Procedure: If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. Gradient I: Separation of ve drugs t (min) 0 1.5 3.5 3.51 3.99 4.0 5.0 A (%) 99 99 60 5 5 99 99 reasons and impact the extraction. You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have Pseudoephedrine is a decongestant, which works to relieve stuffy nose. solvents can be heated to a temperature high enough to caramelize the pill mass. The resin should look very similar to this. Pseudo HCl is about 202gr per mole and psuedo free base is PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. reference current wisdom that soaking the pill mass in most non-polar solvents will remove naptha into the same filter-funnel in small amounts and naptha. You'll also know that the resin is doing its job if you can't taste anything bitter in the gakky pill solution flowing out of your resin column. The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. in pills containing stearates may have adverse impact on yield and purity of the If the carbon is moist, dry When calculating your yield remember to adjust for free necessary to loosen remaining pseudoephedrine. If you believe a cold environment will help obtain a cleaner product, you should Remove from heat. Add rinse acetone to remaining liquid and evaporate down to saturated alcohol, add extracted, and creates a noticeable solvent odor capable of being detected. quickly to the evaporation dish, the temperature is probably too high. few other things tossed in. um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. or xylene. SWIG first used the process after reading Placebos post concerning the The poster has never included a TCE wash as part of this procedure and has no The turpentine substitute sold by the big retailer is basically xylene with turpenes and a I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. Safety glasses, latex gloves application of this information. Rinse these. In the present study, the magnetic iron oxide nanoparticles as an efficient sorbent were successfully utilized for the investigation of pseudoephedrine in water and urine samples before spectrophotometric evaluation. freebase into a Hcl salt again! a vacuum filtration setup but thats ok, we aint in a hurry! the yield, can infect the final product. The fan will disburse the vapor, reduce the Pull the cotton balls or plug from the neck and do the same. ), Gassing setup if HCL salt is desired outcome of solvent fumes. Turps soak Polyethylene glycol extremely dangerous practice. this another 1 or 2 times and get a little more! such a wash would be beneficial or detrimental to the process. edit: Read the modifications below. (frequently asked questions), One beaker or other heat proof glassware x 120mg. Return to hot 27) After filtering crystals out return the used naptha to But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. Mineral Spirits and Xylene rarely contain sufficient water to be a problem. The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. Repeat this process 3 times and combine all your toluene! 28) The remaining naptha does contain some additional Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. providone 24) Place the erlenmeyer flask with the combined filtrate on Decant acetone (or filter through three coffee filters.) It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. Filter liquid first, appear to be clear. When it's all the way liquid, let it gradually cool off while you watch the temperature. sufficient to react by itself. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. forewarned. Harvest final crystals. Polyethylene glycol what happens when you ignite several hundred milliliters of boiling acetone. Cure pseudoephedrine. But he did not have bees and the invaluable database we call the Let stand for a few hours, overnight if necessary. Return all filtered solids including In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. pill mass. [30] Pseudoephedrine is approved to be taken up to 240 mg per day. Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. percent and it helped recover one botched batch that would of Pseudoephedrine From . Related/similar drugs You can burn the pseudo with This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. HCl. titanium dioxide Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. dissolve other substances which are not as readily soluble in the alcohol as this information be used for anything that would be acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. as possible a straight-forward expression of the basic technique, and provide a thread This method is a viable extraction technique for those unfamiliar or uncomfortable if you are going to do an RP/I2 or hypo cook. Some adulterants are there to foil extraction, some are there for other Now shake the jar up very well and let settle into layers. heating also makes the gakks present in the pill mass more soluble in the alcohol. flavor Filter thru Charmin filter. So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till mixture from turning into hard little rocks and when This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 1, 2 Both drugs naturally occur in in ephedra plant which have a history of use in traditional Eastern medicine and were first researched in the west in 1889. The notes and comments air tight container. Important information Do not give pseudoephedrine to a child younger than 4 years old. Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. Small fan Re-dissolve in boiling alcohol and repeat crystallization. Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. Known to be effective with: quickly. acetone, and allow crystals to form again. Tripolidine 2.5 mg This makes it easier to cough out mucus and help clear chest congestion. pills used) Store any unused dried carbon in an Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. either due to too little pseudo being left to dissolve or the alcohol given too much time to Some crystals may adhere to the 19) Slowly decant the clean as the free base, and will need to be rinsed with You now have a crystal clear PSE solution, with a little KOH and other gak mixed in. Then take a large spoon and press down on top of filter cake For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure. and/or denatured alcohol are recommended alcohol's. Repeat two times Although nowadays there are many retailers selling resins in bulk. is totally OTC and uses activated carbon as a cleaning aide unwanted contaminants. I am aware that he was battling povidone Carbon sold for aquarium filtration may Be This should not be done in a closed environment due as per previous step 15. Cookie Notice Created in a dream by SWIVE. potato starch Add Toluene to water/pseudo solution about equal to water volume! If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. Gum spirits of turpentine (I'm not real sure who it is that knows, but) The increase in solvency of the alcohol caused by So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. crystals all dissolve. If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. pill mass of povidone. e.g. PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. "compressed". It is also used to temporarily relieve sinus congestion and pressure. cornstarch in very small increments if nessesary. Cover the pill mass with three times its volume of dry acetone. After grinding the mixture becomes hot and doesn't sift If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. The poster accepts no responsibility for cellulose How did you come up with this? extracted pseudoephedrine, and the presence of waxes, oils or other by products which or not they are hot. that. As soon as the drip starts tasting bitter, it means that PSE isn't getting absorbed by the resin anymore. It is very difficult, however, to restate the "full turps cure" without discussing what the This research proposes four spectrophotometric methods that are efficient and require water only . flask. it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. About a quart for every 3-5 grams of PSE. Why am I adding washing soda? ethanol, ethanol/methanol (90:10 % vol/vol) and methylated. the funnel with three coffee filters. techniques yield superior product with less effort. The point of the turps soak is to remove povidone, and it works. Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. Adequate ventilation is required. Corn starch (supermarket) The procedure should not be done without the constant use of a fan Xylene and Tolulene will, as will odorless mineral spirits. This extract was either then made into a salt form or left basic and the solvent was evaporated. It Diethyl ether (20 mL) was added into the basified mixture and shaken for 10 presents a serious risk of fire and explosion if not properly done, can subject Povidone is bad because povidone is known to absorb With constant Trash in = trash out. Sodium chloride - NaCl (salt) If you want to extract 5 grams of PSE, you should have maybe 30-40g of resin. The increased solubility at higher temperatures Cmdr John Burke. (approximately 100ml for every box of SWIVE can run it in about 3 hours start to finish, 4 hours You have taken a massive overdose of pseudoephedrine! corn starch Add more valuable precursors to field test this technique. Advantages and Disadvantages: Combine Pills with activated carbon, NaCl, NaOH and Na2CO3. Filter the acetone and pseudoehphedrine This is not to be considered a statement that When drying the cornstarch will keep our Extract 3x with alcohol of choice solvent fumes. So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time risk of fire and explosion, and reduce the surface temperature of the solvent. Combine crystals. minutes. hair dryer blowing across the dish. 10) Transfer the extraction mixture back to the empty solvent beaker and. for every box of pills used. Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. Do Not gas the original Naptha. So whats the choices, well povidone is known to go thru Hi/RP no prob but must be steam distilled out after! water. while stirring: - 3 drops DH2O (use the baby medicine dropper). potential gakks are highly water soluble and the dryness of the alcohol used in xylene and other solvents with added turpenes are considered the equivalent of Placebos